Open Access

Development and Characterization of Bio-Hybrid Composites Reinforced with Sansevieria cylindrica, Bamboo Fibers, Areca Sheath Powder, and ZnO Nanoparticles

N. Devendran, nmdev24@gmail.com
Department of Civil Engineering, Saveetha School of Engineering, Saveetha Institute of Medical and Technical Sciences, Chennai, TN, India
T. S. Lakshmi lakshmits.sse@saveetha.com
Department of Civil Engineering, Saveetha School of Engineering, Saveetha Institute of Medical and Technical Sciences, Chennai, TN, India



J. Environ. Nanotechnol., Volume 14, No 3 (September 2025) pp. 338-353

https://doi.org/10.13074/jent.2025.09.2531733

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Abstract

This work seeks to develop advanced hybrid composites utilizing compression molding and hand layup techniques. To improve mechanical and dynamic mechanical properties, the composites incorporate 1-3wt% Areca sheath powder and ZnO nanoparticles, reinforced with 20wt% Sansevieria cylindrica and Bamboo fibers. Dynamic analysis for natural frequency and damping factor, tensile testing, impact testing, modulus measurements, and Fourier transform infrared spectroscopy (FTIR) were employed to assess the behaviour of the composites. The identification of functional groups and chemical bonds was enabled by Fourier transform infrared spectroscopy. The mechanical testing demonstrated significant improvements. The tensile strength of the S7-type composite sample arise from 23.13 to 133.11 MPa, while the tensile modulus increased from 2.83 to 15.07 GPa. The S7 composite exhibited superior elastic and viscous properties, as indicated by storage modulus of 2220 MPa and loss modulus 120 MPa, according to the dynamic mechanical analysis (DMA) results. The combined effects of Areca sheath powder, ZnO nanoparticles, and natural fibers resulted in improved performance in flammability tests for S7-type composites, achieving a heat release rate of 104.05 kW/m2 and a total heat release of 183.39 MJ/m2. Furthermore, vibration analysis identified a natural frequency of 101 Hz for the S7-type composites, signifying enhanced structural stability and energy dissipation. The findings suggest that these hybrid composites may be used in various domains, including construction, infrastructure, aerospace, marine and the automotive industries.

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Reference


Al-Lhaibi, S. A. and Al-Shabander, B. M., Study the effect of ZnO nanoparticles reinforced sawdust /epoxy composites on mechanical properties, Dig. J. Nanomater. Biostruct., 17(3), 851–860(2022).

https://doi.org/10.15251/DJNB.2022.173.851

Barczewski, M., Sałasińska, K., Raś, W., Hejna, A., Michałowski, S., Kosmela, P., Aniśko, J., Boczkowska, A. and Szostak, M., The effect of hybridization of fire retarded epoxy/flax-cotton fiber laminates by expanded vermiculite: Structure-property relationship study, Adv. Ind. Eng. Polym. Res., 6(2), 181–194(2023).

https://doi.org/10.1016/j.aiepr.2023.01.005

Chen, J., Gu, S., Li, W., Yuan, Z. and Cheng, H., Effects of NaOH alkali treatment concentration on the properties of moso bamboo strips and their epoxy resin composites, Nongye Gongcheng Xuebao/ Trans. Chin. Soc. Agric. Eng., 38(15), 234–240(2022).

https://doi.org/10.11975/j.issn.1002-6819.2022.15.025

Diharjo, K., Gapsari, F., Andoko, A., Wijaya, M. N., Mavinkere Rangappa, S. and Siengchin, S., Flammability and thermal resistance of Ceiba petandra fiber-reinforced composite with snail powder filler, Polym. Compos., 45(6), 4947–4960 (2024).

https://doi.org/10.1002/pc.28100

Giridharan, K., Sasirekha, S., Padmanabhan, S., Chakravarthi, G. and Stalin, B., Effect of green pea pod lignin addition on thermal degradation, flame resistance, DMA, and creep resistance of pineapple fibre epoxy composite, Biomass Convers. Biorefin., 14(23), 29843–29852(2024).

https://doi.org/10.1007/s13399-023-04841-2

Gupta, R. K., Mayakannan, S., Vijayaraghavalu, S., Poornima, M. M., Nanthakumar, S. and Bhaskaran, N. A., Multi-objective Optimization of Bamboo-madar Fiber Reinforced Composites for Lightweight Automotive Applications using Machine Learning and Genetic Algorithms, J. Environ. Nanotechnol., 13(4), 358–376(2024).

https://doi.org/10.13074/jent.2024.12.244978

Harak, S. S., Krishnaveni, K., Karthick, K., Chinnarasu, K., Prasad, V. H. P., Tonk, A. and Mayakannan, S., Experimental Study on the Mechanical Properties of Hybrid Areca and Abaca Fiber Reinforced Polymer Composites, J. Environ. Nanotechnol., 13(4), 92–101(2024).

https://doi.org/10.13074/jent.2024.12.244977

Iyyadurai, J., Arockiasamy, F. S., Manickam, T., Rajaram, S., Suyambulingam, I. and Siengchin, S., Experimental Investigation on Mechanical, Thermal, Viscoelastic, Water Absorption, and Biodegradability Behavior of Sansevieria Ehrenbergii Fiber Reinforced Novel Polymeric Composite with the Addition of Coconut Shell Ash Powder, J. Inorg. Organomet. Polym. Mater., 33(3), 796–809(2023).

https://doi.org/10.1007/s10904-023-02537-8

Khan, M. K. A., Faisal, M. and Prakash, V. R. A., Effect of silane coupling grafted polyethylene terephthalate foam and areca fruit fiber reinforced chitin modified vinyl ester prosthetic composite on thermal and water accelerated aging conditions, Polym. Compos., 45(6), 5111–5124(2024a).

https://doi.org/10.1002/pc.28114

Khan, M. K. A., Faisal, M. and Prakash, V. R. A., Characterization of sea urchin spike chitin macromolecule and basalt-encapsulated bamboo fiber-epoxy environmental friendly composite for human prosthetic application, Polym. Bull., 81(12), 10767–10785(2024b).

https://doi.org/10.1007/s00289-024-05208-x

Krishnasamy, B., Thirugapillai, P., Rajakannu, A. and Selvaraju, M., Optimization and multi-objective analysis of tensile, flexural and impact strength in nano-hybrid bio-composites reinforced with Helicteres isora, Holoptelea integrifolia fibers, and nanographene, Revista Materia, 30, 240864(2025).

https://doi.org/10.1590/1517-7076-RMAT-2024-0864

Kumar, R. and Chauhan, S., Effect of ammonium polyphosphate as synergist with nano silica dioxide on flammability of boron compound pretreated bamboo flour-HDPE composite, Fire Saf. J., 133, 103647(2022).

https://doi.org/10.1016/j.firesaf.2022.103647

Kumar, R., Gunjal, J. and Chauhan, S., Effect of borax-boric acid and ammonium polyphosphate on flame retardancy of natural fiber polyethylene composites, Maderas: Ciencia y Tecnologia, 24, 1-10(2022).

http://dx.doi.org/10.4067/s0718-221x2022000100434

Lan, X., Bian, C., Yang, Y., Zhang, Q. and Huang, G., Modified Epoxy Resin on the Burning Behavior and Mechanical Properties of Aramid Fiber, Compos. Mater, 17(16), 4028(2024).

https://doi.org/10.3390/ma17164028

Li, W., Zhang, L., Chai, W., Yin, N., Semple, K., Li, L., Zhang, W. and Dai, C., Enhancement of flame retardancy and mechanical properties of polylactic acid with a biodegradable fire-retardant filler system based on bamboo charcoal, Polym., 13(13), 2167(2021).

https://doi.org/10.3390/polym13132167

Manickaraj, K., Ramamoorthi, R., Sathish, S. and Makeshkumar, M., Effect of hybridization of novel African teff and snake grass fibers reinforced epoxy composites with bio castor seed shell filler: Experimental investigation, Polym. Polym. Compos., 30, 2288(2022).

https://doi.org/10.1177/09673911221102288

Narayanan, L. and Muthukumaran, S., Development of silane-treated corn husk fiber and agro-waste biofiller-reinforced epoxy composite: effects on wear, mechanical, thermal, and water absorption properties, Biomass Convers. Biorefin., 14(23), 30801–30817 (2024).

https://doi.org/10.1007/s13399-024-05837-2

Ngouobe, J. N., Lecompte, T., Ngohe-Ekam, P. S., Nfornkah, B. N., Bailleul, J. L., Kervoelen, A., Magueresse, A., Bastianelli, F., Noah, P. M. A., Kanmogne, A., Bayeck, A. J. P. and Szczepaniak, R., Comparative study of the physical and mechanical properties of Bambusa vulgaris fibers from Cameroon for application to hybrid composite materials, Ind. Crops Prod., 222(3), 119725(2024).

https://doi.org/10.1016/j.indcrop.2024.119725

Pachiappan, A. and Santhanam, S. K. V., Mechanical behavior of snake grass fiber with neem gum filler hybrid composite, Polimeros, 33(3), 0033(2023).

https://doi.org/10.1590/0104-1428.20220116

Palanisamy, S., Kalimuthu, M., Dharmalingam, S., Alavudeen, A., Nagarajan, R., Ismail, S. O., Siengchin, S., Mohammad, F. and Al-Lohedan, H. A., Effects of fiber loadings and lengths on mechanical properties of Sansevieria cylindrica fiber reinforced natural rubber biocomposites, Mater. Res. Exp., 10(8), 85503(2023).

https://doi.org/10.1088/2053-1591/acefb0

Ponnuswamy, M., Sathishkumar, T. P., Selvaraju, M. and Sundramurthy, V. P., Enset ventricosum Fibre-Based Biocomposite Preparation with Wood Apple Shell Particles as a Filler: Effect of Alkali Treatment and Optimization of Composition for Physio-Mechanical Properties, Arabian J. Sci. Eng., 49(11), 15733–15748(2024).

https://doi.org/10.1007/s13369-024-09253-6

Prabhu, P., Karthikeyan, B., Ravi, R. M. V. R. and Balaji, A., Investigation on mechanical, dynamic mechanical analysis, thermal conductivity, morphological analysis, and biodegradability properties of hybrid fiber mats reinforced HLCE resin nanocomposites, Polym. Compos., 43(12), 8850–8859(2022).

https://doi.org/10.1002/pc.27066

Raja, T. and Devarajan, Y., A novel way of converting waste-enriched composites to lightweight, biodegradable resources: a property analysis, Biomass Convers. Biorefin., 14(16), 19431–19441(2024).

https://doi.org/10.1007/s13399-023-03872-z

Raja, T., Devarajan, Y., Patel, G. M., Nath, J. K., Kalidhas, A. M., Sharma, S. and Chaudhary, P., Sustainable enhancement of Henequen fiber-reinforced polymer composites with copper oxide nanoparticles: A step forward in clean engineering and technology, Cleaner Eng. Technol., 27, 101039(2025).

https://doi.org/10.1016/j.clet.2025.101039

Ramadoss, P. K., Mayakrishnan, M. and Arockiasamy, F. S., Discarded custard apple seed powder waste-based polymer composites: an experimental study on mechanical, acoustic, thermal and moisture properties, Iran. Polym. J., 33(4), 461–479(2024).

https://doi.org/10.1007/s13726-023-01266-6

Saha, A., Kulkarni, N. D., Kumar, M. and Kumari, P. (2024). The structural, dielectric, and dynamic properties of NaOH-treated Bambusa tulda reinforced biocomposites—an experimental investigation, Biomass Convers. Biorefin., 14(20), 26247–26266(2024).

https://doi.org/10.1007/s13399-023-04709-5

Sasaki, S., Naito, K. and Uchidate, M. Development of polylactic acid-untreated bamboo filler composite and its chemical and mechanical properties, J. Appl. Polym. Sci., 141(23), 55461(2024).

https://doi.org/10.1002/app.55461

Sathish, K. R., Vandhana, D. V., Nivedhitha, D. M., Srish, S. S., Visakan, S., Bharath, S. S. and Sathish, K. S. B. Effect of nanoparticles in natural fiber reinforced polymer composites, Mater. Today: Proc., 20266(2023).

https://doi.org/10.1016/j.matpr.2023.04.130

Singh, S., Singh, A. and Sharma, S. K. Analytical Prediction Models for Density, Thermal Conductivity and Mechanical Strength of Micro-scaled Areca Nut Powder-Reinforced Epoxy Composites, J. Inst. Eng. India Ser. C, 101(1), 43–51(2020).

https://doi.org/10.1007/s40032-019-00535-9

Subramaniam, B., Manickavasagam, V. M., Rajakumar I, P. T., Raj, P. A. C., Bharath, V. G., Madhusudhanan, J., Sharma, A. K., Patil, P. and Assefa, G. B., Investigation of Mechanical Properties of Sansevieria cylindrica Fiber/Polyester Composites, Adv. Mater. Sci. Eng., 6(1), 2180614(2022).

https://doi.org/10.1155/2022/2180614

Torres, M., Rodriguez, V. R., Alcantara, P. I. and Franco-Urquiza, E., Mechanical properties and fracture behaviour of agave fibers bio-based epoxy laminates reinforced with zinc oxide, J. Ind. Text., 51(4), 5847S-5868S(2022).

https://doi.org/10.1177/1528083720965689

Velmurugan, G., Chohan, J. S., Kumar, G., Shankar, V. S. and Nagaraj, M., Innovative building thermal insulation: bamboo fiber-based eco-composite with eggshell powder and cardboard waste reinforcement, J. Balkan Tribol. Assoc., 31(3), 388–408(2025).

Velmurugan, G., Babu., K., Nagaraj, M. and Kumar, A. J. P., Investigations of Flame Retardancy, Mechanical and Thermal Properties of Woven Hemp/PP Hybrid Composite for Insulating Material Reinforced with Synthetic Silicon and Zinc Oxides, Silicon, 15(11), 4875–4888(2023).

https://doi.org/10.1007/s12633-023-02408-4

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