Open Access

Evaluating the Material Performance of AZ91 Reinforced with 3 wt. % of Nano SiC and Micro B4C Through Stir Casting

J. Allen Jeffrey, jeffyresearch@gmail.com
Department of Mechanical Engineering, Loyola Institute of Technology, Chennai, TN, India
V. Sivaraman, vsivaramancbe@gmail.com
Department of Mechanical Engineering, Sri Muthukumaran Institute of Technology, Chennai, TN, India
S. Suresh Kumar, sandysureesh@gmail.com
Department of Mechanical Engineering, PERI Institute of Technology, Mannivakkam, Chennai, TN, India
D. Srinivasan, dsrinivasanseenu2020@gmail.com
Department of Mechanical Engineering, Loyola Institute of Technology, Chennai, TN, India
S. Joshika, joshisri2805@gmail.com
Department of Mechanical Engineering, Loyola Institute of Technology, Chennai, TN, India
J. Nithish, nithish.j2004@gmail.com
Department of Mechanical Engineering, Loyola Institute of Technology, Chennai, TN, India
R. Yuvaraj, ryuvaraj776@gmail.com
Department of Mechanical Engineering, Loyola Institute of Technology, Chennai, TN, India
T. Lokesh lokeshmaran09@gmail.com
Department of Mechanical Engineering, Loyola Institute of Technology, Chennai, TN, India



J. Environ. Nanotechnol., Volume 14, No 3 (September 2025) pp. 371-378

https://doi.org/10.13074/jent.2025.09.2531601

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Abstract

This research employs the stir-casting approach to cast magnesium AZ91 with micro boron carbide (µ-B4C) and nano silicon carbide (n-SiC) ceramics individually at a 3 wt.% concentration, aiming for the successful fabrication of a composite with defect-free production. This approach is chosen because magnesium is valued for its lightweight nature. Still, its weak mechanical traits restrict its broader use. Each sample's properties are tested in different ways, evaluating the integrity of the material by physical characterization, such as density and porosity measurement. A metallurgical assessment was done to investigate the microstructural dispersion of reinforcement in the composite. Mechanical properties, including flexural and impact strength, were analyzed to evaluate their resistance performance subjected to stress conditions. Salt spray tests were performed to assess the material's performance in corrosive environments. To investigate how much wear loss has occurred, a pin-on-disc is utilized. These investigations helped clarify how the composite may be used with various sorts of applications and highlights the promise of uses in engineering sectors that call for lightweight materials with exceptional performance.

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Reference


Ahmadian, H., Zhou, T., Alansari, A., Kumar A. S., Fathy, A., Elmahdy, M., Yu, Q., and Weijia, G., Microstructure, mechanical properties and wear behavior of Mg matrix composites reinforced with Ti and nano SiC particles, J. Mater. Res. Technol., 31, 4088-4103(2024).

https://doi.org/10.1016/j.jmrt.2024.07.125

Alam, M. T., Ahmad, T., Alshoaibi, A. M., Aziz, A., Husain, D. and Ahmad, S., Comprehensive Study on the Properties of AZ91/x-Si3N4 Composites for Their Prospective Application, Appl. Sci., 14(11), 4444 (2024).

https://doi.org/10.3390/app14114444

Amalan, P. A. and Sivaram, N. M., A state-of-the-art review on magnesium-based composite materials, Adv. Mater. Process. Technol., 9(3), 760-778(2022).

https://doi.org/10.1080/2374068X.2022.2096835

Ayyanar, S., A. Gnanavelbabu., K. Rajkumar., P. Loganathan., and K. Vishal., Investigation on microstructure and tribological performance of zirconium boride reinforced AZ91D magnesium alloy: effect of processing routes, Proc. Inst. Mech. Eng., Part C: J. Mech. Eng. Sci., 237(3), 692-707 (2023).

https://doi.org/10.1177/09544062221125058

Baraniraj, A., Sathiyagnanam, A. P., Venkatesh, R. and Aravind, R., Silicon carbide particle enriched magnesium alloy (AZ91) composite: physical, microstructural and mechanical studies, Silicon, 15(15), 6367-6374 (2023).

https://doi.org/10.1007/s12633-023-02516-1

Efe, G. A., The Production of B4C Reinforced Metal Matrix Composite from Waste AZ91 Magnesium Alloy Using the Ball Milling Method, J. New Results Sci., 13(1), 36-46(2024).

https://doi.org/10.54187/jnrs.1461923

Erarslan, Y. and Cem, A., Wear behavior of AZ91D magnesium composite, Sigma J. Eng. Nat. Sci., 33(3), 465-471(2015).

https://doi.org/en/pub/sigma/issue/65751/1021936

Huang, S. J., Diwan, M. S., Subramani, M. and Chiang, C. C., Microstructure evaluation, quantitative phase analysis, strengthening mechanism and influence of hybrid reinforcements (β-sicp, bi and sb) on the collective mechanical properties of the AZ91 magnesium matrix, Met., 11(6), 898(2021).

https://doi.org/10.3390/met11060898

Huang, S. J., Adityawardhana, Y. and Sanjaya, J., Predicting mechanical properties of magnesium matrix composites with regression models by machine learning, J. Compos. Sci., 7(9), 347 (2023).

https://doi.org/10.3390/jcs7090347

Jeffrey, J. A., Kumar, S. S., Roseline, V. A., Mary A. L. and Santhosh, D., Contriving and Assessment of Magnesium Alloy Composites Augmented with Boron Carbide VIA Liquid Metallurgy Route, Mater. Sci. Forum., 1048, 3–8(2022a).

https://doi.org/10.4028/www.scientific.net/msf.1048.3

Jeffrey, J. A., Kumar, S. S., Hariharan, P., Kamesh M. and Raj, A. M., Production and Assessment of AZ91 Reinforced with Nano SiC through Stir Casting Process, Mater. Sci. Forum., 1048, 9–14(2022b).

https://doi.org/10.4028/www.scientific.net/msf.1048.9

Karthik, R., Sankaran, N. S., Venkatesh Raja, K. and Venkatesh, R., Synthesis and characteristics evaluation of magnesium alloy (AZ91) nanocomposite developed with ZrO2 via liquid state stir cast process, Sādhanā, 48(3), 188 (2023).

https://doi.org/10.1007/s12046-023-02243-8

Kumar, A., Kumar, S. and Mukhopadhyay, N. K., Introduction to magnesium alloy processing technology and development of low-cost stir casting process for magnesium alloy and its composites, J. Magnesium Alloys., 6(3), 245-254(2018).

https://doi.org/10.1016/j.jma.2018.05.006

Kumar, T. S., Shalini, S., Ramu, M. and Govindaraju, M., Characterisation of AZ31/ZrO2 composites produced via stir casting, Mater. Res. Express., 6(11), 1165d1(2019).

https://doi.org/10.1088/2053-1591/ab4eae

Kumar, A., Kumar, S., Mukhopadhyay, N. K., Yadav, A. and Winczek, J. Effect of SiC Reinforcement and Its Variation on the Mechanical Characteristics of AZ91 Composites, Mater., 13(21),4913 (2020).

https://doi.org/10.3390/ma13214913

Kumar, A., Kumar, S., Mukhopadhyay, N. K., Yadav, A., Kumar, V. and Winczek, J., Effect of variation of SiC reinforcement on wear behaviour of AZ91 alloy composites, Mater., 14(4), 990(2021).

https://doi.org/10.3390/ma14040990

Liu, B., Yang, J., Zhang, X., Yang, Q., Zhang, J. and Li, X., Development and application of magnesium alloy parts for automotive OEMs: A review. Journal of Magnesium and Alloys, 11(1), 15-47 (2023).

https://doi.org/10.1016/j.jma.2022.12.015

Ma, G., Xiao, H., Ye, J. and He, Y., Research status and development of magnesium matrix composites, Mater. Sci. Technol., 36(6), 645-653(2020).

https://doi.org/10.1080/02670836.2020.1732610

Murali, V. K. and Starvin, M. S., Experimental study on hybrid magnesium composites for human bone implants. Journal of the Chilean Chemical Society, 68(3), 5911-5917 (2023).

http://dx.doi.org/10.4067/s0717-97072023000305911

Nami, B., Razavi, H., Mirdamadi, S., Shabestari, S. G. and Miresmaeili, S. M., Effect of Ca and rare earth elements on impression creep properties of AZ91 magnesium alloy, Metall: Mater. Trans. A., 41(8), 1973-1982(2010).

https://doi.org/10.1007/s11661-010-0238-y

Pooja, K., Tarannum, N. and Chaudhary, P., Metal matrix composites: revolutionary materials for shaping the future, Discov Mater, 5(1), (2025).

https://doi.org/10.1007/s43939-025-00226-6

Rahmany, G. R., Alizadeh, A. and Jafari, H., Microstructure and mechanical properties of stir cast ZX51/Al2O3p magnesium matrix composites, Mater. Sci. Eng A., 674, 413-418(2016).

https://doi.org/10.1016/j.msea.2016.07.057

Rajkumar, S., Loganathan, M. and Venkatesh, R., Optimization of NACL based spray corrosion test process parameters of heat-treated hybrid metal matrix composites, Bull. Chem. Soc. Ethiop., 36(4), 903-914 (2022).

https://dx.doi.org/10.4314/bcse.v36i4.15

Rajak, D. K. and Menon, A., Insights into Magnesium Alloy Significance, J. Alloys Metall. Syst., 9, 100158 (2025).

https://doi.org/ 10.1016/j.jalmes.2025.100158

Santhosh, M. S., Natrayan, L., Kaliappan, S., Patil, P. P., Rao, Y. S., Kumar, T. S., Dhanraj, J. A. and Paramasivam, P., Mechanical and Wear Behaviour of Nano‐Fly Ash Particle‐Reinforced Mg Metal Matrix Composites Fabricated by Stir Casting Technique, J. Nanomater., 2022(1), 5465771(2022).

https://doi.org/10.1155/2022/5465771

Sharma, A., Nagarajan, N., Srinivasan, S. K., Kannan, S., Soudagar, M. E. M., Fouly, A. and Seikh, A. H., Investigational studies on characteristics of Nano Silicon Nitride Incorporated AA8050 composites, Matéria (Rio de Janeiro), 30, e20240779 (2025).

https://doi.org/10.1590/1517-7076-RMAT-2024-0779

Tan, J. and Ramakrishna, S., Applications of magnesium and its alloys: A review, Appl. Sci., 11(15), 6861(2021).

https://doi.org/10.3390/app11156861

Zhang, J., Miao, J., Balasubramani, N., Cho, D. H., Avey, T., Chang, C. Y. and Luo, A. A., Magnesium research and applications: Past, present and future, J. Magnesium Alloys., 11(11), 3867-3895(2023).

https://doi.org/10.1016/j.jma.2023.11.007

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