Synthesis and Characterization of Pure and Copper-doped HAp Nanoparticles by Microwave Irradiation Method
J. Environ. Nanotechnol., Volume 9, No 3 (2020) pp. 01-06
Abstract
Hydroxyapatite (HAp) is a nano biomaterial incorporated as bone and teeth implants in the human body. In the present work, HAp was prepared using calcium hydroxide as a calcium source and orthophosphoric acid as a phosphorous source by chemical co-precipitation method associated with microwave irradiation method. Pure and copper-doped HAp nanoparticles were synthesized by chemical co-precipitation method associated with microwave irradiation method. The prepared copper-doped HAp was characterized by XRD, FTIR, SEM, EDAX, UV and PL techniques. The X-ray Diffraction (XRD) pattern had revealed the crystalline size of the nanoparticles. The Fourier Transform Infrared Spectroscopy (FTIR) pattern had given the functional groups. Morphology and purity of the sample were analyzed by Scanning Electron Microscopy (SEM) and Energy Dispersion X-ray Diffraction (EDAX). The optical properties were ascertained by using Ultra-Violet spectroscopy (UV) and Photo Luminance spectroscopy (PL). The results obtained matched well with the standard values.
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