Open Access

Synthesis and Characterization of Pure Tin Oxide and Magnesium-doped Tin Oxide Nanoparticles by Chemical Precipitation Method

S. Kavitha, kavivp12@gmail.com
Department of Physics, Navarasam Arts & Science College for Women, Arachalur, Erode, TN, India.
S. Sasikala, Department of Physics, Navarasam Arts & Science College for Women, Arachalur, Erode, TN, India. V. Kalaiselvi, Department of Physics, Navarasam Arts & Science College for Women, Arachalur, Erode, TN, India. V. Ramya Department of Physics, Navarasam Arts & Science College for Women, Arachalur, Erode, TN, India.


J. Environ. Nanotechnol., Volume 9, No 3 (2020) pp. 24-28

https://doi.org/10.13074/jent.2020.09.203414

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Abstract

Magnesium-doped tin oxide (SnO2) nanoparticles were synthesized by the chemical precipitation method. This comes under bottom-up approach. The obtained results of metal oxide nanoparticles were characterized by XRD, FTIR, SEM, EDAX, UV and PL, respectively. The average grain size was calculated from XRD spectrum, which confirms the crystalline nature. Then the presence of functional groups was determined using Fourier Transform Infrared spectroscopy (FTIR), and surface morphology and particle size examinations were carried out by Scanning electron microscope (SEM). The purity and elemental composition of the sample were identified from EDAX. Finally, the optical properties and bandgap energy were analyzed by using UV-Visible spectroscopy and PL. It was concluded from the results that the samples synthesized were suitable for the application of dye degradation.

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Reference


Alivisatos, A. P., Semiconductor Clusters, Nanocrystals, and Quantum Dots, Science, 271(5251), 933-937(1996).

https://doi.org/10.1126/science.271.5251.933

Kumari, N., Ghosh, A., Tewari, S. and Bhattacharjee, A.,Synthesis, structural and optical properties of Al doped SnO2 nanoparticles, Ind. J. Phys., 88(1), 65–70(2014).

https://doi.org/10.1007/s12648-013-0387-0

Monredon, S. D., Cellot, A., Ribot, F., Sanchez, C., Armelao, L., Gueneau, L. and Delattre, L., Synthesis and characterization of crystalline tin oxide nanoparticles, J. Mater. Chem., 12(8), 2396-2400(2002).

https://doi.org/10.1039/B203049G

Morales, J. and Sanchez, L., Electrochemical behaviour of SnO2 doped with boron and indium in anodes for lithium secondary batteries, Solid State Ionics, 126(3-4), 219-226(1999).

https://doi.org/10.1016/S0167-2738(99)00251-9

Nayral, C., Viala, E., Fau, P., Senocq, F., Jumas, J.C., Maisonnat, A. and Chaudret, B., Synthesis of tin and tin oxide nanoparticles of low size dispersity for application in gas sensing, Chem. A Eur. J., 6(22), 4082(2000).

https://doi.org/10.1002/1521-3765(20001117)6:22<4082::AID-CHEM4082>3.0.CO;2-S

NurulSyahidahSabri, MohdSallehMohdDeni, AzlanZakaria and Mahesh Kumar Talari., Effect of Mn Doping on Structural and Optical Properties of SnO2 Nanoparticles Prepared by Mechanochemical, Processing Physics Procedia, 25, 233 – 239(2012).

https://doi.org/10.1016/j.phpro.2012.03.077

Wang, Y. and Lee, J. Y., Preparation of SnO2 graphite nanocomposites anodes by ureamediated hydrolysis, Electrochem. Commun., 5(4), 292-296(2003).

https://doi.org/10.1016/S1388-2481(03)00035-3

Warnken, M., Lazark, K. and Wark, M., Redox behaviour of SnO2 nanoparticles encapsulated in the pores of zeolites towards reductive gas atmospheres studied by in situ diffuse reflectance UV/Vis and Mossbauer spectroscopy, Phys. Chem. Chem. Phys., 3(10), 1870-1876(2001).

https://doi.org/10.1039/B009045J

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