Green Synthesis of Psidium guajava Capped Hydroxyapatite Nanoparticles
J. Environ. Nanotechnol., Volume 9, No 3 (2020) pp. 19-23
Abstract
The current research focuses on the synthesis and characterization of hydroxyapatite nanoparticles of 26±5 nm size from Psidium guajava leaf extract with control over dimensions and composition. The reaction occurred very rapidly as the formation of spherical nanoparticles was almost completed within 30 nm. The probable pathway of the green synthesis was suggested. Appearance, crystalline nature, size and shape of the nanoparticles were examined by Scanning Electron Microscopy, Energy Dispersive X-Ray Analysis, Fourier Transform Infrared Spectroscopy and X-Ray Diffraction techniques. A microwave-assisted route was selected for the synthesis of hydroxyapatite nanoparticles to carry out the reaction fast, suppress the enzymatic action and keep the process environmentally clean and green.
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Reference
Frasnelli, M., Cristofaro, F., Sglavo, V. M., Dirè, S., Callone, E., Ceccato, R., Bruni, G., Cornaglia, A. I. and Visai, L., Synthesis and characterization of strontium-substituted hydroxyapatite nanoparticles for bone regeneration, Materials Science and Engineering: C., 71(1), 653-662(2017).
https://doi.org/10.1016/j.msec.2016.10.047
Gopi, D., Kanimozhi, K., Bhuvaneshwari, N., Indira, J. and Kavitha, L., Novel banana peel pectin mediated green route for the synthesis of hydroxyapatite nanoparticles and their spectral characterization, Spectrochimica Acta Part A, Molecular and Biomolecular Spectroscopy, 118(24), 589-597(2014).
https://doi.org/10.1016/j.saa.2013.09.034
Kalaiselvi, V., Mathammal, R. and Anitha, P., Sol-gel mediated synthesis of pure hydroxyapatite at different
temperatures and silver substituted hydroxyapatite for biomedical applications, J. Biotechnol. Biomater., 7(275), 2(2017).
https://doi.org/10.4172/2155-952X.1000275
Kalaiselvi, V., Mathammal, R., Vidhya, N. and Surya, K., Synthesis and Characterization of Pure and Capped Hydroxyapatite Nanoparticles, Int. J. Adv. Sci. Eng., 6(1), 1213-1219(2019).
https://doi.org/10.29294/IJASE.6.1.2019.1213-1219
Kalaiselvi, V., Mathammal, R., Vijayakumar, S. and Vaseeharan, B., Microwave assisted green synthesis of Hydroxyapatite nanorods using Moringa oleifera flower extract and its antimicrobial applications, Int. J. Vet. Sci. Med., 6(2), 286-295(2018).
https://doi.org/10.1016/j.ijvsm.2018.08.003
Kalaiselvi V, Mathammal R. Synthesis and Characterization of Pure and Triethanolamine Capped Hydroxyapatite Nanoparticles and its Antimicrobial and Cytotoxic Activities, Asian J. Chem., 30(8), 1696-1700(2018).
https://doi.org/10.14233/ajchem.2018.21214
Kumar GS, Rajendran S, Karthi S, Govindan R, Girija E.K, Karunakaran G, Kuznetsov D. Green synthesis and antibacterial activity of hydroxyapatite nanorods for orthopedic applications, MRS Communications, 7(2), 183-188(2017).
https://doi.org/10.1557/mrc.2017.18
Sundrarajan, M., Jegatheeswaran, S., Selvam, S., Sanjeevi, N. and Balaji, M., The ionic liquid assisted green synthesis of hydroxyapatite nanoplates by Moringa oleifera flower extract: a biomimetic approach, Materials & Design, 88, 1183-1190(2015).
https://doi.org/10.1016/j.matdes.2015.09.051
Vasant, S. R. and Joshi, M. J., Synthesis and characterization of pure and zinc doped calcium pyrophosphate dihydrate nanoparticles, Eur. Phys. J. Appl. Phys., 53(1), 10601(2011).
https://doi.org/10.1051/epjap/2010100095
Yuan, Q., Wu, J., Qin, C., Xu, A., Zhang, Z., Lin, Y., Chen, Z., Lin, S., Yuan, Z., Ren, X. and Zhang, P., One-pot synthesis and characterization of Zn-doped hydroxyapatite nanocomposites, Materials Chemistry and Physics, 199:122-130(2017).
