Open Access

Growth, Spectral, Structural and Thermal Properties of Inorganic Materials TetrabutylammoniumTetrabromoCobaltate (II) Crystal

R. Umarani, grishchandru@yahoo.com
Department of Chemistry, Government Arts College (Autonomous), Coimbatore, TN, India.
V. Mohanraj, Department of Chemistry, SRMV College of Arts and Science (Autonomous), Coimbatore, TN, India. M. Thenmozhi, Centre for Nanotechnology and Advanced Biomaterials, SASTRA University, Thanjavur, TN, India. M. A. Kandasamy Department of Chemistry, SRMV College of Arts and Science (Autonomous), Coimbatore, TN, India.


J. Environ. Nanotechnol., Volume 4, No 2 (2015) pp. 65-74

https://doi.org/10.13074/jent.2015.03.152146

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Abstract

Single crystals of Tetrabutylammoniumtetrabromocobaltate (II) crystal, was grown by slow evaporation method at room temperature. The crystals belong to a class of compounds that shown interesting properties like phase transitions and ferroelectric behaviour in a narrow temperature. The grown crystals were characterized through elemental analysis, powder X-ray diffraction, thermogravimetric analysis, differential thermal analysis, low temperature differential scanning calorimetry techniques. The spectral studies of FTIR, 1H and 13C NMR spectra were obtained for the sample. Single crystal X-ray diffraction technique is used to find the structure and crystal packing of the compounds.

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Reference


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