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Journal of Environmental Nanotechnology

(A Quarterly Peer-reviewed and Refereed International Journal)
ISSN(Print):2279-07 48; ISSN(Online):2319-5541
CODEN:JENOE2

Review Article

Impact of Reducing Agent on the Synthesis of Nickel Oxide Nanoparticles by Chemical Precipitation Method

V.Kayathri 1,  K.Kousalya 2,  A.Mafeena 3,  M.Monisha 4,  S.Naga Nandhini 5,  J.Balavijayalakshmi 6*.  

Corresponding Author Email: balavijayalakshmiroopa@gmail.com

This article has not yet been cited.

1, 2, 3, 4, 5, 6. Department of Physics, PSGR Krishnammal College For Women, Coimbatore, Tamilnadu, India.


Abstract

This present work reports the synthesis ad characterization of Nickel oxide nanoparticles by chemical precipitation method from nickel chloride by using two different reducing agents, such as ammonia (NH3) and sodium hydroxide (NaOH). The prepared nanoparticles are characterized by X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), Field Emission-Scanning Electron Microscopy (FE-SEM) and Energy Dispersive X-ray analysis (EDAX) techniques. XRD analysis showed that the prepared nanoparticles are crystalline in nature, and the average crystallite size for NiO nanoparticles with NaOH and NiO nanoparticles with NH3 is found to be 25.3 nm and 27.54 nm, respectively. FE-SEM analysis revealed that the prepared nanoparticles are spherical in shape with agglomeration. The presence of functional groups of the prepared nanoparticles is confirmed by using FT-IR analysis. The band at 450 cm-1 corresponds to the stretching vibration on Ni-OH, which confirms the presence of NiO, and the elemental analysis confirms the presence of nickel and oxygen elements in the prepared nickel oxide nanoparticles without any Impurities. The synthesized nickel oxide nanoparticles may be used in micro-supercapacitors, electrochromic coatings, and chemical sensing devices.


J. Environ. Nanotechnol., Volume 10, No. 1. 14-18
ISSN: 2279-0748 eISSN: 2319-5541
ENT211432.pdf
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Reference

Ali, A. A., El Fadaly, E. and Ahmed, I. S., Near-infrared reflecting blue inorganic nano-pigment based on cobalt aluminate spinel via combustion synthesis method, Dyes and Pigments, 158, 451-462(2018).

doi:10.1016/j.dyepig.2018.05.058

 

Bhavani, P., Rajababu, C., Arif, M., Reddy, I. V. S. and Reddy, N. R., Synthesis of high saturation magnetic iron oxide nanomaterials via low temperature hydrothermal method, J. Magn. Magn. Mater., 426(C), 459-466(2017).

doi:10.1016/j.jmmm.2016.09.049

Ganachari, S. V., Bhat, R., Deshpande, R. and Venkataraman, A., Synthesis and characterization of nickel oxide nanoparticles by self-propagating low temperature combustion method, Recent Research in Science and Technology, 4(4), 50-53(2012).

Gandhi, A. C., Cheng, H. Y., Chang, Y. M. and Lin, J. G., Size confined magnetic phase in NiO nanoparticles, Mater. Res. Express., 3(3), 035017(2016).

doi:10.1088/2053-1591/3/3/035017

Ibraheem, F., Aziz, M. H., Fatima, M., Shaheen, F., Syed Mansoor Ali and Huang, Q., In vitro cytotoxicity, MMP and ROS activity of green synthesized nickel oxide nanoparticles using extract of Terminalia chebula against MCF-7 cells, Mater. Lett., 234 (1), 129–133(2019).

doi:10.1016/j.matlet.2018.09.075

Kavitha, B., Nirmala, M. and Pavithra, A., Annealing effect on nickel oxide nanoparticles synthesized by sol-gel method, World Scientific News, 52, 118-129(2016).

Lassoued, A., Lassoued, M. S., Dkhil, B., Ammar, S., Gadri, A., Synthesis, photoluminescence and Magnetic properties of iron oxide (α-Fe2O3) nanoparticles through precipitation or hydrothermal methods, Physica E: Low-dimensional Systems and Nanostructures, 101, 212-219(2018).

doi:10.1016/j.physe.2018.04.009

Lingaraju, K., Raja Naika, H., Nagabhushana, H. and Nagaraju, G., Euphorbia heterophylla (L.) mediated fabrication of ZnO NPs: Characterization and evaluation of antibacterial and anticancer properties, Biocatal. Agri. Biotech., 18, 100894(2019).

doi:10.1016/j.bcab.2018.10.011

Nassar, M. Y., Aly, H. M., Abdelrahman, E. A., Moustafa, M. E., Synthesis, characterization and biological activity of some novel Schiff bases and their Co(II) and Ni(II)complexes: a new route for Co3O4 and NiO nanoparticles for photocatalytic degradation of methylene blue dye, J. Mol. Struct., (1143), 462–471(2017).

doi:10.1016/j.molstruc.2017.04.118

Patil, P. S. and Kadam, L. D., Preparation and characterization of spray pyrolyzed nickel oxide (NiO) thin films, Applied Surface Science, 199(1-4), 211-221(2002).

doi:10.1016/S0169-4332(02)00839-5

Shanmuagpriya, T. and Balavijayalakshmi, J., Preparation and characterization of nitrogen doped graphene oxide/nickel oxide nanocomposites for dye sensitized solar cell applications, Adv. Appl. Res., 11(1), 34-38(2019).

doi:10.5958/2349-2104.2019.00006.8

Singh, P., Kim, Y. J., Zhang, D., Yang, D. C.,  Biological synthesis of nanoparticles from plants and microorganisms, Trends Biotechnol., 34(7), 588–599(2016).

doi:10.1016/j.tibtech.2016.02.006

Sone, B. T., Fuku, X. G., Maaza, M., Physical and electrochemical properties of green synthesized bunsenite NiO nanoparticles via Callistemon viminalis extracts, Int. J. Electrochem. Sci., 11, 8204–8220(2016).

doi: 10.20964/2016.10.17

Sun, D. L., Zhao, B. W., Liu, J. B., Wang,  H. and Yan, H., Application of nickel oxide nanoparticles in electrochromic materials, Ionics, 23(6), 1509-1515(2017).

doi:10.1007/s11581-017-1974-4

Taghizadeh, F., The study of structural and magnetic properties of NiO nanoparticles, Optics and Photonics Journal, 6(8), 164-169(2016).

doi:10.4236/opj.2016.68B027

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